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erbium(III) Chloride

ErCl3 salt

Properties

StateSolid (hygroscopic; commonly hydrated)
Colorpink
SolubilityVery soluble in water; soluble in alcohols
Melting Point807 °C (anhydrous)

About erbium(III) Chloride

Erbium(III) chloride is the soluble Er entry point — that distinctive deep-pink hexahydrate ErCl3·6H2O is what you actually pull off the shelf, because the anhydrous chloride is a hygroscopic nightmare to keep dry. The pink color is f-f electronic transitions of Er3+ around 522, 540, and 654 nm; it's intense enough that a centimolar aqueous solution looks like dilute cranberry juice. As with the rest of the heavy lanthanide chlorides, simple thermal dehydration in air goes the wrong way — you lose HCl preferentially over H2O above 200 °C and end up with ErOCl, not anhydrous ErCl3. The clean preparations are the same as for DyCl3: NH4Cl-assisted dehydration at 300 °C under inert gas, vacuum sublimation around 800 °C, or direct synthesis from Er metal turnings plus dry HCl. The crystallographic punchline is the same too — anhydrous ErCl3 takes the AlCl3 layered structure with 6-coordinate Er3+, while in aqueous solution the [Er(H2O)8]3+ aqua ion (8-coordinate, square antiprism) dominates because Er3+ is small enough to start losing one inner-sphere water relative to the lighter lanthanides. The chemistry that makes Er3+ commercially indispensable is its 4I13/2 → 4I15/2 transition at 1530 nm, which sits exactly in the C-band telecom window and made the entire modern optical-fiber backbone possible. ErCl3 is the typical wet-chemistry starting point for Er-doped phosphors, Er:YAG laser crystal precursors, and Er-doped optical-fiber preforms.

Where you'll encounter it

If you've ever fed an Er-doped sol-gel synthesis or made a precursor solution for an Er-doped fluoride fiber preform, you started by dissolving ErCl3·6H2O in deionized water or methanol — the pink color tells you immediately whether you've hit the right concentration. In a dental or dermatology clinic, the practical product downstream of ErCl3 is the Er:YAG laser at 2.94 µm — the wavelength sits on the OH-stretch absorption peak of water, so the laser ablates enamel or skin in 5 µm slices with almost no thermal collateral. In a research telecom lab, ErCl3 is the precursor for MCVD (modified chemical vapor deposition) Er-doped fiber preforms that get drawn into the EDFA gain fibers used in every undersea cable repeater.

Common Uses

  • Precursor for Er-doped silica and ZBLAN fluoride glass fiber amplifiers (EDFAs)
  • Wet-chemistry starting material for Er:YAG laser crystal feedstock preparation
  • Dopant source for green and red upconversion phosphors in Er/Yb systems
  • Feedstock for Er metal production by molten chloride electrolysis
  • Lewis acid catalyst for selected aldol and Mannich reactions
  • Reagent for Er3+ separations from Ho and Tm via solvent extraction
  • NMR shift reagent precursor for paramagnetic chemical shift work
  • Pink colorant in specialty optical glass and ceramic glaze formulations

Safety Information

GHS H315/H319 (skin and eye irritation, Category 2/2A). The hexahydrate is mildly acidic in solution (pH ~4 for 0.1 M) and releases small amounts of HCl as it deliquesces in humid air — handle in a fume hood with nitrile gloves. Acute toxicity is moderate (LD50 ~3-5 g/kg). No specific OSHA PEL; treat as a soluble lanthanide salt with respirable dust limit of 5 mg/m3. As with all rare-earth chlorides, chronic occupational inhalation has been linked to pulmonary fibrosis in refinery cohorts.

This safety summary is for educational reference only and may not be complete. It is not a substitute for Safety Data Sheets (SDS), medical advice, or professional chemical safety guidance. Always consult appropriate SDS and qualified professionals before handling chemicals.

Constituent Elements

Frequently Asked Questions

What is the molar mass of erbium(III) chloride?
273.61 g/mol for anhydrous ErCl3 (167.26 for Er + 3 × 35.45 for Cl). The hexahydrate ErCl3·6H2O — what you actually buy — is 381.71 g/mol. As with DyCl3, double-check whether your supplier lists anhydrous or hydrated mass on the COA, because the 28% mass difference will throw off any stoichiometric synthesis.
Why is Er:YAG used in dentistry?
The Er:YAG emission at 2.94 µm sits almost exactly on the strongest OH-stretch absorption peak of liquid water, giving an absorption coefficient around 12,000 cm^-1. That means optical penetration of only 3-5 µm into hydrated tissue (enamel is ~10% water, dentin is ~25%). Each pulse vaporizes a thin layer too fast for heat to conduct into surrounding tissue, so you get precision ablation with minimal thermal damage and often no need for local anesthesia. The same wavelength is the workhorse of fractional skin resurfacing in dermatology for the same reason.
Why is anhydrous ErCl3 hard to prepare?
Direct thermal dehydration of ErCl3·6H2O in air loses HCl preferentially over H2O above ~200 °C and gives ErOCl plus HCl gas instead of the desired ErCl3. The clean syntheses are NH4Cl-assisted dehydration (heat the hydrate with a 6:1 molar excess of NH4Cl at 300 °C — the NH4Cl·HCl adduct sublimes off and leaves anhydrous ErCl3), vacuum sublimation at 800 °C, or direct synthesis from Er metal turnings plus dry HCl gas at 300-400 °C. The product picks up moisture faster than CaCl2, so it goes straight into a glove box.