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Gold(III) Chloride

AuCl3 salt

Properties

StateSolid
ColorRed-brown to dark red
SolubilitySoluble in water (hydrolyzes); soluble in ethanol and HCl
Melting Point254 °C (decomposes)

About Gold(III) Chloride

Gold(III) chloride is a red-brown crystalline solid that doesn't actually exist as the AuCl3 monomer in any condensed phase — it dimerizes to Au2Cl6, a planar molecule with two square-planar Au(III) centers bridged by two chlorides, like the structure of Al2Cl6 but with d⁸ Au(III) demanding square-planar geometry instead of tetrahedral. That d⁸ preference for square-planar coordination is the same one that drives Pd(II) and Pt(II) chemistry, and it's the structural motif that makes Au(III) catalysis interesting in organic synthesis. AuCl3 hydrolyzes rapidly in water and dissolves in HCl to give the tetrachloroaurate anion [AuCl4]⁻, isolated commercially as the yellow-orange chloroauric acid HAuCl4·3H2O — the form that >90% of gold-on-the-shelf reagent chemistry actually uses. Reduce HAuCl4 with sodium citrate in boiling water and you get the famous wine-red colloid of 10-20 nm gold nanoparticles via the Turkevich method; citrate first reduces Au(III) to Au(0) and then coordinates the nanoparticle surface to keep them from aggregating. Those colloids are what you see as the red line on a COVID lateral-flow test, the surface-enhanced Raman scattering substrates for trace molecule detection, and the photothermal absorbers in research-stage cancer treatments where nanoparticles concentrate in tumors and release heat under near-infrared illumination. AuCl3 is also seeing growing use as a homogeneous catalyst for alkyne hydration and gold-carbene-mediated C-H functionalization, chemistry that won Hashmi and Toste a lot of attention in the late 2000s.

Where you'll encounter it

If you've ever taken a rapid antigen test (COVID, pregnancy, strep), the colored line that shows up was made of gold nanoparticles synthesized from chloroauric acid — typically 20-40 nm spheres conjugated to antibodies, which migrate up the strip with the sample and concentrate at the test line if the analyte is present. In a nanoparticle synthesis lab running the Turkevich citrate method, you bring 100 mL of 0.25 mM HAuCl4 to a vigorous boil, inject 5 mL of 1% sodium citrate, and watch the wine-red color stabilize in five to ten minutes as 10–20 nm spheres nucleate. In a homogeneous gold-catalysis lab studying alkyne hydration, AuCl3 at 1–5 mol% in wet methanol gives Markovnikov hydration without needing the heavier Hg(II) catalysis that ruled the field before Hashmi's papers.

Common Uses

  • Precursor for gold nanoparticle synthesis (Turkevich citrate method)
  • Source of nanoparticles for lateral-flow rapid diagnostic test lines
  • Au(III) catalyst for alkyne hydration and hydroarylation reactions
  • Starting material for gold electroplating bath formulations
  • Photothermal nanoparticle precursor for research-stage cancer therapy
  • Reagent for SERS (surface-enhanced Raman scattering) substrate fabrication
  • Historical photographic toner for albumen and silver-gelatin prints

Safety Information

GHS: Acute toxicity oral Category 4 (H302, harmful if swallowed), skin corrosion/irritation Category 2 (H315), serious eye irritation Category 2A (H319). Soluble Au(III) salts cause contact dermatitis ('gold rash') in sensitized individuals — about 1-2% of dental workers develop it from gold restoration alloys. Chronic systemic exposure causes chrysiasis, a permanent blue-gray skin discoloration from sub-dermal Au(0) deposits formed by photoreduction of accumulated gold. OSHA has no specific PEL. Practical handling: wear nitrile gloves (Au(III) won't permeate latex but will stain the skin), work in a hood when manipulating powder to avoid inhalation, and keep separate from cyanides (the [Au(CN)4]⁻ complex is far more bioavailable than [AuCl4]⁻). Aqueous solutions slowly photoreduce in sunlight to colloidal gold — store HAuCl4 stocks in amber glass.

This safety summary is for educational reference only and may not be complete. It is not a substitute for Safety Data Sheets (SDS), medical advice, or professional chemical safety guidance. Always consult appropriate SDS and qualified professionals before handling chemicals.

Constituent Elements

Frequently Asked Questions

What is the molar mass of gold(III) chloride?
AuCl3 weighs 303.32 g/mol: gold (196.967) + 3 chlorines (3 × 35.45 = 106.35). The reagent you actually buy is almost always the trihydrate of chloroauric acid, HAuCl4·3H2O, which weighs 393.83 g/mol — a 30% mass difference. If a procedure says '50 mg AuCl3' and you weigh out 50 mg of HAuCl4·3H2O, you're actually using 25% less gold than the protocol calls for, which matters in nanoparticle synthesis where size depends sharply on Au:reductant ratio.
What's the difference between AuCl3 and HAuCl4?
AuCl3 is the anhydrous binary chloride (actually existing as the dimer Au2Cl6 in solid and gas phase). HAuCl4 is chloroauric acid, formed when AuCl3 dissolves in HCl: AuCl3 + HCl → HAuCl4. The acid is far easier to handle — water-soluble (>500 g/L), forms stable yellow-orange crystalline trihydrate HAuCl4·3H2O, doesn't hydrolyze rapidly. Almost every nanoparticle synthesis paper, electroplating bath formulation, and gold-catalysis protocol that says 'gold chloride' is actually using HAuCl4·3H2O. Anhydrous AuCl3 is reserved for moisture-sensitive organometallic chemistry where chloride speciation matters.
How does the Turkevich method make gold nanoparticles?
Bring 100 mL of 0.25 mM HAuCl4 to a vigorous boil in a clean flask, inject 5 mL of 1% sodium citrate, watch over the next 5-10 minutes as the solution turns gray (Au(0) clusters nucleating), then dark blue (aggregates), then transitions to wine-red as 10-20 nm spherical particles stabilize. Citrate plays both roles: a 3-electron reductant per molecule (oxidizing to acetone-1,3-dicarboxylate plus CO2) reducing Au(III) to Au(0), and an electrostatic capping ligand whose carboxylate groups coordinate the nanoparticle surface and prevent aggregation through Coulombic repulsion. Particle size tunes from 5-150 nm by adjusting the citrate-to-gold ratio.