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Oxalic Acid

C2H2O4 organic

Properties

StateSolid at room temperature
ColorWhite crystalline powder
SolubilitySoluble in water (14.3 g/100 mL at 25 °C)
Melting Point189 °C (decomposes)

About Oxalic Acid

Oxalic acid is the simplest dicarboxylic acid, written HOOC-COOH, with a molar mass of 90.034 g/mol. The two carboxyl groups sit directly on each other, which makes the first ionization unusually strong for an organic acid (pKa1 = 1.25, comparable to bisulfate) and gives the dianion (oxalate) excellent bidentate chelating geometry — a five-membered ring closes when oxalate binds a metal through both carboxylate oxygens. This chelation is why oxalic acid eats rust: it pulls Fe(III) out of iron oxide and ferries it away as the soluble tris(oxalato)ferrate(III) complex. Plants store oxalic acid as the calcium salt — those needle-like raphide crystals in spinach, rhubarb leaves, and dieffenbachia are calcium oxalate, and the same insoluble salt is what kidney stones are mostly made of. In a chemistry teaching lab, oxalic acid is the primary standard for KMnO4 titrations: the reaction 5 C2O4^2- + 2 MnO4- + 16 H+ yields 10 CO2 + 2 Mn^2+ + 8 H2O is self-indicating because the purple permanganate color disappears as soon as it's reduced, returning at the endpoint when oxalate is exhausted. The reaction needs to run hot (about 60 °C) and slowly at first because it is autocatalyzed by Mn(II).

Where you'll encounter it

If you've ever stripped iron stains from a porcelain sink, restored an old wooden deck, or watched a beekeeper sublime acid crystals into a hive to kill Varroa mites, you've used oxalic acid. Wood-deck cleaners sold at hardware stores are often 5-10 percent oxalic acid solutions because the chelation chemistry pulls tannins and iron stains out of cedar and redwood without bleaching the lignin. In analytical labs, sodium oxalate (Na2C2O4, NIST SRM 40) is still the gold-standard primary reference for permanganate standardization in undergraduate quant courses. Industrial chemists exploit oxalate's bidentate chelation in rare-earth separation, where oxalate precipitation is one of the cleanest ways to remove lanthanides from solution before calcining the oxalates to mixed oxides for further processing.

Common Uses

  • Rust and iron-stain removal from porcelain, wood decks, and stone via Fe(III) chelation
  • Bleaching and brightening agent for wood pulp, restored furniture, and textile fibers
  • Primary standard for standardizing potassium permanganate solutions in analytical chemistry
  • Reducing agent in classic redox titrations and in Tollens-type silver-mirror experiments
  • Sublimed in beehives at low doses for Varroa mite control by hobbyist and commercial beekeepers

Safety Information

Toxic if ingested. Lethal oral dose in adults is around 15-30 g. Once absorbed, oxalate precipitates with serum calcium as insoluble calcium oxalate, causing hypocalcemia, kidney damage, and tubular obstruction. Corrosive to skin and mucous membranes. GHS: H302 (harmful if swallowed), H312 (harmful in contact with skin), H318 (causes serious eye damage). The airborne dust carries a low occupational exposure limit. Wear nitrile gloves, splash goggles, and dust mask when weighing dry crystals, and never mouth-pipette solutions.

This safety summary is for educational reference only and may not be complete. It is not a substitute for Safety Data Sheets (SDS), medical advice, or professional chemical safety guidance. Always consult appropriate SDS and qualified professionals before handling chemicals. We deliberately do not publish occupational exposure limits or other regulatory thresholds: those values are revised over time and differ between jurisdictions, so the only correct source is the current SDS and the regulations that apply where you work.

Constituent Elements

Frequently Asked Questions

What is the molar mass of oxalic acid?
The molar mass of anhydrous oxalic acid (C2H2O4) is 90.034 g/mol from 2 carbon (24.022) + 2 hydrogen (2.016) + 4 oxygen (63.996). The dihydrate form sold commercially (C2H2O4 . 2 H2O, 126.07 g/mol) is what you actually weigh out in lab — be careful with this when standardizing titrants, because the two waters are part of the formula weight you put on the balance.
Why is oxalic acid used in KMnO4 titrations?
Three reasons. First, the reaction is self-indicating — purple MnO4- bleaches as it oxidizes oxalate, and the first persistent pink at the endpoint marks completion. Second, sodium oxalate is available as a NIST primary standard with five-nines purity, so you can weigh out a known mass and trust the moles. Third, the stoichiometry is clean: 5 C2O4^2- + 2 MnO4- + 16 H+ yields 10 CO2 + 2 Mn^2+ + 8 H2O. Run it at 60 °C and add the first few drops slowly because the reaction is autocatalyzed by Mn(II).
What foods contain oxalic acid?
Spinach, rhubarb leaves (the petioles are safer), beet greens, Swiss chard, sorrel, cocoa, cashews, and dark teas. Spinach contains roughly 750 mg per 100 g, mostly as calcium oxalate raphides. People prone to calcium-oxalate kidney stones are usually advised to pair high-oxalate foods with calcium so the oxalate precipitates in the gut rather than being absorbed. Rhubarb leaves contain enough free oxalate to be genuinely toxic — the stalks people actually eat contain far less.