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Cobalt(II) Nitrate

Co(NO3)2 salt

Properties

StateSolid (crystalline, deliquescent)
ColorDeep red to magenta (hexahydrate); pale red (anhydrous)
SolubilityHighly soluble in water (1030 g/L at 20°C)
Melting Point55°C (hexahydrate); 100°C (decomposes, anhydrous)
Boiling PointDecomposes before boiling

About Cobalt(II) Nitrate

Cobalt(II) nitrate is the deliquescent magenta hexahydrate that catalyst chemists reach for when they need a clean cobalt source. The reason is straightforward: the nitrate counterion decomposes thermally to N2 and O2 in the temperature window 100–300 °C, leaving behind pure cobalt oxide with no chloride poisoning, no sulfur residues, and no carbon coke. That's why Co(NO3)2·6H2O is the standard precursor for Fischer-Tropsch catalyst preparation (cobalt impregnated on alumina or silica, calcined to Co3O4, then reduced to metallic Co⁰ for CO+H2 chemistry to liquid hydrocarbons), and for cobalt-zeolite catalysts used in selective NH3-SCR of NOx emissions in lean-burn diesel exhaust. The hexahydrate has [Co(H2O)6]²⁺ octahedra in the solid state and stays in that octahedral coordination in dilute aqueous solution — same magenta color as the chloride hexahydrate, same d-d transitions around 510 nm. Rinmann's green test exploits its qualitative-analysis behavior: dab a chip of suspected zinc compound with cobalt nitrate solution, ignite in a flame, and zinc oxide reacts with cobalt oxide at high temperature to form the spinel CoZnO2 (Rinmann's green), confirming zinc presence with a distinctive green color. The same chemistry made cobalt nitrate the historical reagent of choice for testing aluminum and magnesium minerals — Thénard's blue (CoAl2O4) for aluminum, pink CoMgO2 for magnesium. As a strong oxidizer, it ignites paper and organic solvents on contact when concentrated.

Where you'll encounter it

If you've ever prepared a supported cobalt catalyst by incipient-wetness impregnation, you weighed out Co(NO3)2·6H2O (the hexahydrate is the only form that comes off the shelf — the anhydrous decomposes too readily in air), dissolved it in just enough water to fill the pore volume of your alumina support, then calcined at 400 °C to drive off NO2 and water. The slow weight loss as nitrate decomposes is a clean marker on a TGA trace, which is one reason it's still preferred over the acetate or chloride for catalyst-prep procedures.

Common Uses

  • Precursor for Fischer-Tropsch cobalt-on-alumina catalysts in coal-to-liquids and gas-to-liquids plants
  • Wet-impregnation cobalt source for NH3-SCR catalysts treating diesel-engine NOx emissions
  • Pickling-bath additive in nickel-cobalt electroplating formulations targeting gold-color decorative finishes
  • Rinmann's green qualitative test reagent identifying zinc by forming CoZnO2 spinel after ignition
  • Thénard's blue (CoAl2O4) preparation for ceramic underglaze and stained-glass coloration
  • Sympathetic-ink demonstrations for K-12 chemistry showing reversible Oh/Td color change on heating
  • Cathodic dye source for cobalt-pink ceramic glazes fired below 1100 °C to prevent black-spinel formation
  • Calibration standard in ICP-OES at 228.6 nm cobalt emission line for trace metals analysis

Safety Information

GHS H272 (oxidizer, may intensify fire), H302 (harmful if swallowed), H317 (skin sensitization), H334 (respiratory sensitization with occupational asthma), H341 (suspected mutagen), H350i (carcinogenic by inhalation, IARC Group 2B), H360F (reproductive toxicity), H410 (very toxic to aquatic life). OSHA PEL for cobalt is 0.1 mg Co/m³ as an 8-hour TWA; ACGIH TLV is 0.02 mg/m³. The strong oxidizer behavior is a concrete fire risk: contact between solid Co(NO3)2 and reducing organics like glycerol or paper can ignite spontaneously, and the molten salt above 55 °C is extremely reactive. Store separated from organics in DOT Class 5.1 oxidizer locker. Cobalt sensitization is permanent — once you react to any cobalt salt, exposure to cement dust, hard-metal grinding, or even orthopedic implant wear-debris triggers contact dermatitis.

This safety summary is for educational reference only and may not be complete. It is not a substitute for Safety Data Sheets (SDS), medical advice, or professional chemical safety guidance. Always consult appropriate SDS and qualified professionals before handling chemicals.

Constituent Elements

Frequently Asked Questions

What is the molar mass of cobalt(II) nitrate?
Anhydrous Co(NO3)2 is 182.943 g/mol: cobalt at 58.933 plus two nitrate groups at 62.005 each (each NO3⁻ is 14.007 + 3 × 15.999). The hexahydrate Co(NO3)2·6H2O — which is what's actually on the shelf — is 291.03 g/mol. If a published catalyst-prep procedure asks for X mol of cobalt and you weigh out hexahydrate, divide your gram weight by 291.03, not 182.94.
Why is cobalt nitrate preferred over CoCl2 or CoSO4 for catalyst preparation?
The nitrate anion decomposes thermally between 100 °C and 300 °C to give N2, O2, and NOx — no carbon, no sulfur, no halide residues. Chloride from CoCl2 poisons noble-metal sites and corrodes downstream reactor steel. Sulfate from CoSO4 leaves behind Co3O4 contaminated with surface sulfate that needs aggressive reduction to remove. Acetate decomposes through a carbonate intermediate that can leave coke. Nitrate gives the cleanest Co3O4 endpoint, which is why supported-catalyst recipes overwhelmingly specify the hexahydrate.
How does the Rinmann's green test for zinc actually work?
You moisten a fragment of suspected zinc-containing compound with one or two drops of dilute cobalt nitrate solution, then heat it strongly in an oxidizing flame. The cobalt nitrate decomposes to Co3O4, the zinc compound oxidizes to ZnO, and at red heat the two oxides react in the solid state to form the green spinel CoZnAl2O4 (or CoZnO2 in simpler formulations). The green color is diagnostic for zinc — magnesium gives pink, aluminum gives Thénard's blue (CoAl2O4). Modern qualitative-analysis labs have largely replaced the test with ICP-MS, but it survives in field-mineral-identification kits because it requires only a Bunsen burner and a charcoal block.