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Nickel(II) Sulfate

NiSO4 salt

Properties

StateSolid (crystalline)
ColorYellow-green (anhydrous); emerald green (hexahydrate)
SolubilityHighly soluble in water (650 g/L at 20°C)
Melting Point840°C (anhydrous, decomposes)
Boiling PointDecomposes before boiling

About Nickel(II) Sulfate

Nickel(II) sulfate is the workhorse nickel salt of industry — formula NiSO4, molar mass 154.756 g/mol for the anhydrous form, though you almost never see it anhydrous outside of a calcination furnace. The hexahydrate (NiSO4·6H2O) and heptahydrate (NiSO4·7H2O) are the practical forms, both emerald-green crystals that are extremely water-soluble (650 g/L at 20°C). The compound dominates two industries: nickel electroplating and lithium-ion batteries. In a Watts plating bath, NiSO4·6H2O supplies the bulk of the dissolved nickel — typically 240–340 g/L — with smaller amounts of NiCl2·6H2O for anode activation and boric acid as a pH buffer near 4. The bath runs at 45–60°C and 3–5 A/dm² to deposit decorative-bright or sulfamate-tough nickel onto steel, brass, and zinc die-castings — the matte gray under the chrome on your faucet, the corrosion-resistant flash on copper PCBs, the satin finish inside a tubular musical instrument. The other application is the one rewriting global mining maps: NiSO4 is the precursor for the precipitated mixed hydroxide that becomes the NMC and NCA cathode in every electric-vehicle battery built today, and battery-grade NiSO4 demand is driving roughly $40 billion of new mining and refining capacity in Indonesia, the Philippines, and Australia. NiSO4 is produced by dissolving nickel metal, NiO, or Ni(OH)2 in dilute sulfuric acid.

Where you'll encounter it

If you've ever held a chrome-plated bumper, the bright nickel layer underneath came out of a NiSO4-based Watts bath running 24/7 in a plating shop somewhere — chrome doesn't actually adhere to steel, the bright nickel does, and the chrome is just a 0.25 µm flash on top for color and tarnish resistance. In an analytical lab, NiSO4 is what you grab when you need a soluble Ni²⁺ standard for atomic absorption or ICP-OES calibration. The teaching demo most chemistry undergrads remember is dimethylglyoxime: add a drop of DMG reagent to a Ni²⁺ solution made from NiSO4 and you get a bright cherry-red precipitate that's the textbook example of a chelate complex and the first quantitative test most students perform. Battery industry estimates put NMC cathode demand at over 2 million tonnes per year by 2030, every gram of nickel in those cathodes passes through NiSO4 first.

Common Uses

  • Bulk nickel source in Watts electroplating baths at 240-340 g/L for decorative and engineering plating
  • Battery-grade precursor for NMC and NCA cathode active materials in lithium-ion EV cells
  • Sulfamate nickel bath component for electroforming low-stress thick nickel deposits
  • Soluble Ni²⁺ standard for AA, ICP-OES, and ICP-MS instrument calibration
  • Reagent in the dimethylglyoxime gravimetric test for nickel determination
  • Mordant in the dyeing of wool and nylon with nickel-complex acid dyes
  • Catalyst precursor for nickel-on-silica hydrogenation catalysts in fine-chemical synthesis

Safety Information

GHS classifications: H302 + H332 (harmful if swallowed or inhaled), H315 (skin irritation), H317 (skin sensitization), H334 (respiratory sensitization), H341 (suspected mutagen), H350i (carcinogenic by inhalation), H360D (reproductive toxicity, may damage unborn child), H372 (organ damage with prolonged exposure), H410 (very toxic to aquatic life). IARC Group 1 carcinogen. Occupational exposure limits for soluble nickel compounds are expressed as elemental Ni and are among the lowest applied to common bench salts. EU REACH classifies nickel sulfate as a substance of very high concern (SVHC) for reproductive toxicity. Most common cause of allergic contact dermatitis worldwide. Handle with nitrile gloves, lab coat, splash goggles; weigh in a fume hood. Plating-bath aerosols require local exhaust ventilation and respirator protection. All waste must be collected as heavy-metal hazardous waste.

This safety summary is for educational reference only and may not be complete. It is not a substitute for Safety Data Sheets (SDS), medical advice, or professional chemical safety guidance. Always consult appropriate SDS and qualified professionals before handling chemicals. We deliberately do not publish occupational exposure limits or other regulatory thresholds: those values are revised over time and differ between jurisdictions, so the only correct source is the current SDS and the regulations that apply where you work.

Constituent Elements

Frequently Asked Questions

What is the molar mass of nickel(II) sulfate?
Anhydrous NiSO4 has a molar mass of 154.756 g/mol — nickel at 58.693, sulfur at 32.06, and four oxygens at 15.999 each give 63.996, summing to 154.749 (rounded to 154.756 in most catalogs). The hexahydrate NiSO4·6H2O is 262.847 g/mol and the heptahydrate is 280.862 g/mol. Always check the bottle: most commercial 'nickel sulfate' is the hexahydrate and using the wrong molar mass will skew your formulation by 70%.
Why is nickel sulfate important for electric vehicles?
NiSO4 is the dissolved precursor that goes into the co-precipitation reactor where Ni-Mn-Co hydroxide is grown — the spherical secondary particles that become the NMC cathode after lithiation and calcination. Higher nickel content boosts cell capacity (NMC-811 hits over 200 mAh/g versus ~155 for NMC-111) and replaces expensive cobalt. Battery-grade NiSO4 demand has driven a roughly $40 billion buildout of nickel laterite processing in Indonesia, the Philippines, and Australia over the past five years.
Is nickel sulfate dangerous?
Yes — IARC classifies nickel compounds as Group 1 human carcinogens by inhalation, with strongest evidence for nasal and lung cancer in nickel refinery workers. Occupational exposure limits for soluble nickel compounds are set correspondingly low, as elemental Ni. NiSO4 is also the most common cause of allergic contact dermatitis on Earth — about 17% of women are sensitized, mostly from jewelry and watch backs. Plating shops require respirator-grade ventilation, and any worker with known nickel allergy should avoid handling. EU REACH lists it as an SVHC for reproductive toxicity.